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williamson ether synthesis of phenacetin lab report

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williamson ether synthesis of phenacetin lab report

This is, when an alcohol is combined with an alkyl halide. The liquids involved have to be immiscible, in order to form two distinct layers upon contact. View Lab Report - Lab 6 report from CHE 202 at SUNY Buffalo State College. actual mass that was collected was 1.477g and the percent yield for the synthesis was 71.06%. Lawson 2 Abstract: The objective of the experiment was to synthesize acetaminophen and use it to synthesize phenacetin. Orgo lab Orgo lab Preview text Williamson Ether Synthesis: Preparation of Phenacetin from Acetaminophen Partners: Victor, Zahra April 12, 2016 Methods and Background The goal of this lab is to use the Williamson ether synthesis and prepare a phenacetin. The phenolic hydrogen is sufficiently acidic to be deprotonated by potassium carbonate to allow the reaction to occur. Obtain 360 mg of acetaminophen and transfer into a dry 25-mL round-bottom flask (RBF). Synthesis of Phenacetin from Acetaminophen (Prepared in Lab by Acetylation of -Aminophenol) through Williamson Ether Acetaminophen Lab Report.docx - Synthesis of Phenacetin Abstract In this lab students were able to use Williamson ether synthesis which follows the S 2, In this lab, students were able to use Williamson ether synthesis, which follows the S, mechanism to convert acetaminophen into phenacetin. Williamson Ether Synthesis: Phenacetin from Acetaminophen, Synthesis of Phenacetin From Acetaminophen Experiment.docx, University of Illinois, Chicago • CHEM 233, Queensborough Community College, CUNY • CHEMISTRY 120, Ramapo College Of New Jersey • BIOL 213-01, Yusra Medical and Dental College, Islamabad, Yusra Medical and Dental College, Islamabad • WRI 101, University of British Columbia • CHEM 203. The, purpose of this experiment was to first convert the alcohol to an alkoxide and then carry out a, The percent yield of the synthesis of Phenacetin was 201.2% and, The synthesis of Phenacetin was carried out by a Williamson Ether Synthesis. With the theoretical and experimental yield obtained, the percent yield was calculated and found to be 36.36 %. Acetaminophen is reacted with potassium carbonate and iodoethane to prepare phenacetin via Williamson ether synthesis. Please sign in or register to post comments. By the end of the lab, the phenacetin went through melting point determination to prove whether it was a pure product. Get step-by-step explanations, verified by experts. The potassium carbonate was. After the creation acetaminophen, the. Lab 6 report - Lab 6 Williamson Ether Synthesis of Phenacetin Sara Howard TA Cadnel Sly Detchou March 31st 2015 Abstract In this experiment the, 6 out of 7 people found this document helpful, Lab 6: Williamson Ether Synthesis of Phenacetin, In this experiment, the Williamson ether synthesis of Phenacetin was done by combining. Washing is also used as a step in the, recrystallization procedure to remove the impurity adhering to the crystal surface, Many extractions are based on acid-base chemistry. In this lab, students were able to use Williamson ether synthesis, which follows the S N 2 mechanism to convert acetaminophen into phenacetin. Phenacetin is prepared by taking Acetaminophen, which is an active ingredient in, Tylenol, and mix it with iodoethane in the presence of a base. This preview shows page 1 - 3 out of 10 pages. After the creation acetaminophen, the actual mass that was collected was 1.477g and the percent yield for the synthesis was 71.06%. Most of the extractions are performed using, , in this experiment, 5% NaOH is utilized. The acetaminophen, acted as the nucleophile and the Iodoethane was the electrophile. The atom economy that, was calculated for the synthesis of phenacetin is 0.46289, and this value produced a reaction, In this lab, the main goal was to use the Williamson ether synthesis, this method. The literature and experimental melting point of the acetaminophen are within close range of each other.

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